Ni(C₆H₅PCl₂)4

Base Information

Chemical Name:Ni(C₆H₅PCl₂)4
CAS No.:15675-30-6
Molecular Formula:C₂₄H₂₀Cl₈NiP₄
Molecular Weight:774.632
Hs Code.:

Ni(C<sub>6</sub>H<sub>5</sub>PCl<sub>2</sub>)4

Synonyms:Ni(C₆H₅PCl₂)4

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Chemical Property of Ni(C₆H₅PCl₂)4

Chemical Property:

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Technology Process of Ni(C₆H₅PCl₂)4

There total 2 articles about Ni(C₆H₅PCl₂)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 15675-30-6
Ni(C₆H₅PCl₂)4

Guidance literature:: In neat (no solvent); heating;; pptn.;;

Reference yield:

: 76404-15-4
tetrakis(methyldichlorophosphine)nickel⁽⁰⁾

: 644-97-3
Dichlorophenylphosphine

: 15675-30-6
Ni(C₆H₅PCl₂)4

Guidance literature:: In further solvent(s); byproducts: PCL2CH3; heating soln. of (Ni(PCl2CH3)4) in PCl2C6H5 at 35 Torr for 3 h to 70-80°C (stirring);; removal of excess PCl2C6H5 by vac. distn., residue washed with n-pentane, recrystn. from ether;;
DOI:10.1021/ja01571a020

Reference yield:

: zinc(II) fluoride

: 15675-30-6
Ni(C₆H₅PCl₂)4

: 13987-00-3
{Ni(PF₂C₆H₅)4}

Guidance literature:: In benzene; refluxing ZnF2 and soln. of (Ni(PCl2C6H5)4) in benzene for 4 h in N2-atmosphere, stirring for 10 h at ambient temp.;; pumping off volatile components at 1 torr, dissolving residue in benzene, filtering under N2, concg. in vac., dissolving in ether, treating withactivated carbon, evapg. ether, addn. of petroleum ether, cooling with ice, recrystn., drying in vac.;;