3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

Base Information

Chemical Name:3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile
CAS No.:1202411-80-0
Molecular Formula:C₂₇H₃₄N₄O
Molecular Weight:430.593
Hs Code.:

Synonyms:3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

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Chemical Property of 3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

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Technology Process of 3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

There total 4 articles about 3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-01-3
1-methyl-piperazine

: 1202411-79-7
1-cyano-3-(dibenzylamino)cyclohexanecarboxylic acid

: 1202411-80-0
3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

Guidance literature:: With HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 48.8333h;

Reference yield:

: 1202411-77-5
N,N-dibenzyl-1,5-dichloropentan-2-amine

: 1202411-80-0
3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 79 °C

2.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 16 h / 52 °C

2.2: pH 6

3.1: HATU / N,N-dimethyl-formamide / 48.83 h / 0 - 20 °C

With lithium hydroxide monohydrate; water; caesium carbonate; HATU; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: dibenzyl 2-(dibenzylamino)pentanedioate

: 1202411-80-0
3-(dibenzylamino)-1-[(4-methylpiperazin-1-yl)carbonyl]cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h

2.1: thionyl chloride / toluene / 0.5 h / 20 - 77 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 79 °C

4.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 16 h / 52 °C

4.2: pH 6

5.1: HATU / N,N-dimethyl-formamide / 48.83 h / 0 - 20 °C

With lithium aluminium tetrahydride; thionyl chloride; lithium hydroxide monohydrate; water; caesium carbonate; HATU; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;