methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

Base Information

Chemical Name:methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate
CAS No.:92409-86-4
Molecular Formula:C₂HF₃O₂*C₃₆H₄₈N₈O₈S₂
Molecular Weight:898.982
Hs Code.:

Synonyms:methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

Chemical Property:

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Technology Process of methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

There total 4 articles about methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23446-11-9
tert-butyloxycarbonylmethionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide

: 76-05-1
trifluoroacetic acid

: 92409-86-4
methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

Guidance literature:: With indole; ethandithiol;

Reference yield:

: 23446-03-9
2-((2S)-2-((tert-butoxycarbonyl)amino)-4-(methylthio)butanamido)acetic acid

: 92409-86-4
methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 15.2 g / DCC / dimethylformamide / 1.) 0 deg C, 2 h; 2.) 7-8 deg C, overnight

2: 1.) NEt₃; 2.) HOBt / 1.) DMF, 10 min; 2.) 7-8 deg C, overnight

3: 1.9 g / thioanisole / 1 h / 0 °C

With methyl-phenyl-thioether; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.115

Reference yield:

: 16948-13-3
Boc-Met-OTcp

: 92409-86-4
methionyl-glycyl-tryptophyl-methionyl-aspartyl-phenylalanine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 75.5 percent / Et₃N / H₂O / Ambient temperature

2: 15.2 g / DCC / dimethylformamide / 1.) 0 deg C, 2 h; 2.) 7-8 deg C, overnight

3: 1.) NEt₃; 2.) HOBt / 1.) DMF, 10 min; 2.) 7-8 deg C, overnight

4: 1.9 g / thioanisole / 1 h / 0 °C

With methyl-phenyl-thioether; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.34.115