C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

Base Information

Chemical Name:C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂
CAS No.:1270931-13-9
Molecular Formula:C₁₇H₁₆F₃N₃O₂S₂
Molecular Weight:417.452
Hs Code.:

C<sub>17</sub>H<sub>15</sub><sup>(3)</sup>HF<sub>3</sub>N<sub>3</sub>O<sub>2</sub>S<sub>2</sub>

Synonyms:C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

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Chemical Property of C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

Chemical Property:

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Technology Process of C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

There total 5 articles about C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1270931-20-8
4-iodo-5-(4-methoxytetrahydropyran-4-yl)-2-(4-(3-trifluoromethyl-diazirin-3-yl)phenylthio)thiazole

: 1270931-13-9
C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

Guidance literature:: With tritium; platinum on carbon; triethylamine; In ethyl acetate; at 20 ℃; for 96h; under 200 Torr;
DOI:10.1002/jlcr.1804

Reference yield:

: 1270931-16-2
4-bromo-5-(4-hydroxytetrahydropyran-4-yl)-2-(methylthio)thiazole

: 1270931-13-9
C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 2.5 h / -78 - 20 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1.5 h / 0 °C

4.1: trifluoroacetic anhydride / 0.75 h / 40 °C

5.1: methanol

6.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis(diphenylphosphino)ferrocene; triethylamine / 1-methyl-pyrrolidin-2-one / 16 h / 60 °C / Inert atmosphere; Darkness

7.1: tritium; platinum on carbon; triethylamine / ethyl acetate / 96 h / 20 °C / 200 Torr

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; tritium; 1,1'-bis(diphenylphosphino)ferrocene; platinum on carbon; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In 1-methyl-pyrrolidin-2-one; methanol; diethyl ether; hexane; chloroform; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/jlcr.1804

Reference yield:

: C₉H₁₂INO₂S₂

: 1270931-13-9
C₁₇H₁₅⁽³⁾HF₃N₃O₂S₂

Guidance literature:: Multi-step reaction with 3 steps

1: methanol

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis(diphenylphosphino)ferrocene; triethylamine / 1-methyl-pyrrolidin-2-one / 16 h / 60 °C / Inert atmosphere; Darkness

3: tritium; platinum on carbon; triethylamine / ethyl acetate / 96 h / 20 °C / 200 Torr

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tritium; 1,1'-bis(diphenylphosphino)ferrocene; platinum on carbon; triethylamine; In 1-methyl-pyrrolidin-2-one; methanol; ethyl acetate;
DOI:10.1002/jlcr.1804