5--1,2,3-trimethoxybenzene

Base Information

Chemical Name:5--1,2,3-trimethoxybenzene
CAS No.:120040-61-1
Molecular Formula:C₂₂H₂₂O₃S₂
Molecular Weight:398.547
Hs Code.:

5-<Bis(phenylthio)methyl>-1,2,3-trimethoxybenzene

Synonyms:5--1,2,3-trimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5--1,2,3-trimethoxybenzene

Chemical Property:

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Technology Process of 5--1,2,3-trimethoxybenzene

There total 3 articles about 5--1,2,3-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 882-33-7
diphenyldisulfane

: 120040-61-1
5--1,2,3-trimethoxybenzene

Guidance literature:: With tributylphosphine; In benzene; for 2.5h;
DOI:10.1021/jo00301a026

Reference yield: 42.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 108-98-5
thiophenol

: 120040-61-1
5--1,2,3-trimethoxybenzene

Guidance literature:: With trifluoroacetic acid; In chloroform; at 20 ℃; for 20h;
DOI:10.1002/chem.201600208

Reference yield: 29.0%

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 108-98-5
thiophenol

: 120040-61-1
5--1,2,3-trimethoxybenzene

: 123731-52-2
3,4,5-trimethoxybenzyl phenyl sulfide

Guidance literature:: With oxygen; 9-(2-mesityl)-10-methylacridinium perchlorate; In acetonitrile; at 30 - 35 ℃; for 24h; Schlenk technique; Irradiation;
DOI:10.1039/d0cc02352c