(1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

Base Information

Chemical Name:(1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide
CAS No.:1040919-33-2
Molecular Formula:C₁₅H₁₉NO₂
Molecular Weight:245.321
Hs Code.:

Synonyms:(1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

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Technology Process of (1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

There total 1 articles about (1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1040919-30-9
(3S,3aR,6aS)-3-hydroxy-2-[(1R)-1-phenylethyl]-3,3a,6,6a-tetrahydrocyclopenta[c]pyrrol-1(2H)-one

: 1040919-33-2
(1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

Guidance literature:: With sodium tetrahydroborate; In 1,4-dioxane; water; at 88 ℃; for 5h;
DOI:10.1134/S1070428010040135

Reference yield: 98.0%

: 1040919-33-2
(1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

: 108-24-7
acetic anhydride

: 1240453-80-8
[(1R,5S)-5-{[(1R)-1-phenylethyl]aminocarbonyl}cyclopent-2-en-1-yl]methyl acetate

Guidance literature:: With pyridine; at 20 ℃; for 5h;
DOI:10.1134/S1070428010040135

Reference yield: 90.0%

: 1040919-33-2
(1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide

: 1220043-27-5
(1S,2R,3R)-3-hydroxy-2-(hydroxymethyl)-N-(1-phenylethyl)cyclopentanecarboxamide

Guidance literature:: (1S,2R)-2-(hydroxymethyl)-N-[(1R)-phenylethyl]-cyclopent-3-ene-1-carboxamide; With borane-THF; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; Cooling with ice;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 0.5h;
DOI:10.1016/j.mencom.2010.01.006