diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Base Information

Chemical Name:diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate
CAS No.:180839-04-7
Molecular Formula:C₃₀H₃₆Cl₂N₄O₇
Molecular Weight:635.544
Hs Code.:

diprop-2-enyl N-<(4-<<N-(4-<bis<2-chloroethyl>amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Synonyms:diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

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Chemical Property of diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

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Technology Process of diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

There total 10 articles about diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2067-58-5
4-amino-N,N-bis(2-chloroethyl)aniline

: 180839-04-7
diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0.25 h

2: dibutyltin dilaurate / toluene / 12 h / Ambient temperature

With dibutyltin(II) dilaurate; triethylamine; In dichloromethane; toluene;
DOI:10.1021/jm980425k

Reference yield:

: 18483-99-3
2-(4-nitrobenzyloxy)tetrahydro-2H-pyran

: 180839-04-7
diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 38 percent / ammonium formate / 10 percent Pd/C / ethanol / 1.5 h / 20 °C

2: Et₃N / toluene

3: 45 percent / aq. AcOH / tetrahydrofuran / 3.5 h / 45 °C

4: dibutyltin dilaurate / toluene / 12 h / Ambient temperature

With dibutyltin(II) dilaurate; ammonium formate; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/jm980425k

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 180839-04-7
diprop-2-enyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 1.5 h

2: 38 percent / ammonium formate / 10 percent Pd/C / ethanol / 1.5 h / 20 °C

3: Et₃N / toluene

4: 45 percent / aq. AcOH / tetrahydrofuran / 3.5 h / 45 °C

5: dibutyltin dilaurate / toluene / 12 h / Ambient temperature

With dibutyltin(II) dilaurate; ammonium formate; pyridinium p-toluenesulfonate; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/jm980425k