2-fluorophenyl sulfurofluoridate

Base Information

Chemical Name:2-fluorophenyl sulfurofluoridate
CAS No.:16475-34-6
Molecular Formula:C₆H₄F₂O₃S
Molecular Weight:194.159
Hs Code.:

Synonyms:2-fluorophenyl sulfurofluoridate

Suppliers and Price of 2-fluorophenyl sulfurofluoridate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-fluorophenyl sulfurofluoridate

Chemical Property:

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Technology Process of 2-fluorophenyl sulfurofluoridate

There total 2 articles about 2-fluorophenyl sulfurofluoridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 367-12-4
2-fluorophenol

: 16475-34-6
2-fluorophenyl sulfurofluoridate

Guidance literature:: 2-fluorophenol; With potassium fluoride; potassium carbonate; N,N`-sulfuryldiimidazole; trifluoroacetic acid; In water; acetonitrile;

In water; acetonitrile; at 20 ℃; for 18h;
DOI:10.1021/acs.joc.9b02352

Reference yield:

: 16475-34-6
2-fluorophenyl sulfurofluoridate

Guidance literature:: Aus Thermolyse und Hydrolyse von o-Fluorophenoxythionyltrifluorid;

Reference yield: 87.0%

: 124-38-9,18923-20-1
carbon dioxide

: 16475-34-6
2-fluorophenyl sulfurofluoridate

: 445-29-4
o-fluoro-benzoic acid

Guidance literature:: With manganese; bis(triphenylphosphine)nickel(II) chloride; 2.9-dimethyl-1,10-phenanthroline; In N,N-dimethyl-formamide; at 20 ℃; for 20h; under 760.051 Torr; Schlenk technique; Inert atmosphere; Glovebox;
DOI:10.1021/acs.orglett.9b00836