(S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

Base Information

Chemical Name:(S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid
CAS No.:118943-42-3
Molecular Formula:CH₄O₃S*C₁₄H₁₉F₃N₂O
Molecular Weight:384.42
Hs Code.:

Synonyms:(S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

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Chemical Property of (S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

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Technology Process of (S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

There total 5 articles about (S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 118958-97-7
(S)-6-((S)-1-Phenyl-ethylamino)-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

: 118943-42-3
(S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00163a036

Reference yield:

: 3128-07-2
6-oxoheptanoic acid

: 118943-42-3
(S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 79.7 percent / benzene / 1 h / 50 °C

2: 78.4 percent / 4-(dimethylamino)pyridine, Et₃N / dimethylformamide / 1.5 h / Ambient temperature

4: H₂ / 5percentPd/C / ethanol / 30 h / 60 °C / 3000.2 Torr

With dmap; hydrogen; triethylamine; 5% Pd on active carbon; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/hlca.19880710204

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 118943-42-3
(S)-6-Amino-heptanoic acid (4-trifluoromethyl-phenyl)-amide; compound with methanesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 78.4 percent / 4-(dimethylamino)pyridine, Et₃N / dimethylformamide / 1.5 h / Ambient temperature

3: H₂ / 5percentPd/C / ethanol / 30 h / 60 °C / 3000.2 Torr

With dmap; hydrogen; triethylamine; 5% Pd on active carbon; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710204