2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

Base Information

Chemical Name:2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol
CAS No.:1416371-72-6
Molecular Formula:C₂₃H₃₂N₂O₄
Molecular Weight:400.518
Hs Code.:

Synonyms:2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

Chemical Property:

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Technology Process of 2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

There total 4 articles about 2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 2078-54-8
2,6-diisopropylphenol

: 65673-48-5
4-(2-(2-methoxyethoxy)ethoxyl)aniline

: 1416371-72-6
2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

Guidance literature:: 4-(2-(2-methoxyethoxy)ethoxyl)aniline; With hydrogenchloride; In water;

With sodium nitrite; In water; at 0 ℃; for 0.5h;

2,6-diisopropylphenol; Further stages;
DOI:10.1002/anie.201205475 DOI:10.1002/anie.201205475

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1416371-72-6
2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 750.08 Torr

3.1: hydrogenchloride / water

3.2: 0.5 h / 0 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.201205475 DOI:10.1002/anie.201205475

Reference yield:

: 54149-17-6,92450-98-1
2-bromoethyl 2-methoxyethyl ether

: 1416371-72-6
2,6-diisopropyl-4-((4-(2-(2-methoxyethoxy)ethoxy)phenyl)diazenyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 750.08 Torr

3.1: hydrogenchloride / water

3.2: 0.5 h / 0 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/anie.201205475 DOI:10.1002/anie.201205475