10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane

Base Information

Chemical Name:10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane
CAS No.:938065-20-4
Molecular Formula:C₃₁H₃₂N₂O₃
Molecular Weight:480.607
Hs Code.:

Synonyms:10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane

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Chemical Property of 10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane

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Technology Process of 10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane

There total 2 articles about 10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3558-68-7
2,6-diphenylpyrylium perchlorate

: 84227-51-0
10-phenyl-10-aza-1,4,7-trioxacyclododecane

: 938065-20-4
10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane

Guidance literature:: 2,6-diphenylpyrylium perchlorate; 10-phenyl-10-aza-1,4,7-trioxacyclododecane; In N,N-dimethyl-formamide; at 150 ℃; for 6h;

In diethyl ether;

With ammonium hydroxide; In acetone;
DOI:10.1080/00958972.2018.1434719

Reference yield:

: 120-07-0
2,2'-(phenylimino)bis[ethanol]

: 938065-20-4
10-[4-(2,6-diphenylpyridin-4-yl)phenyl]-1,4,7-trioxa-10-azacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / acetonitrile / 3 h / Inert atmosphere

1.2: Inert atmosphere; Reflux

2.1: N,N-dimethyl-formamide / 6 h / 150 °C

With potassium tert-butylate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/00958972.2018.1434719