1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

Base Information

Chemical Name:1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol
CAS No.:220641-19-0
Molecular Formula:C₃₆H₅₄O₅
Molecular Weight:566.822
Hs Code.:

Synonyms:1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

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Chemical Property of 1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

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Technology Process of 1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

There total 5 articles about 1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17131-52-1,124933-35-3,131064-88-5,131064-87-4
(R)-3-(p-methoxyphenoxy)-1,2-propanediol

: 220641-19-0
1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; dmap / dichloromethane / Ambient temperature

2: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 24 h / Ambient temperature

3: hydrogenchloride; water / 1 h

4: n-butyllithium; potassium hydride

With pyridine; hydrogenchloride; dmap; n-butyllithium; water; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja982837o

Reference yield:

: 220641-16-7
1-O-(triphenylmethyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

: 220641-19-0
1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 24 h / Ambient temperature

2: hydrogenchloride; water / 1 h

3: n-butyllithium; potassium hydride

With hydrogenchloride; n-butyllithium; water; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja982837o

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 220641-19-0
1-O-(1'-octadecynyl)-2-O-(4'-methoxybenzyl)-3-O-(4'-methoxyphenyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 24 h / Ambient temperature

2: hydrogenchloride; water / 1 h

3: n-butyllithium; potassium hydride

With hydrogenchloride; n-butyllithium; water; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja982837o