diphenylthioselenophosphinic acid sodium salt

Base Information

• Chemical Name: diphenylthioselenophosphinic acid sodium salt
• CAS No.: 35351-90-7
• Molecular Formula: C₁₂H₁₀PSSe*Na
• Molecular Weight: 319.201
• Mol file: 35351-90-7.mol

Synonyms:diphenylthioselenophosphinic acid sodium salt

Chemical Property of diphenylthioselenophosphinic acid sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenylthioselenophosphinic acid sodium salt

There total 3 articles about diphenylthioselenophosphinic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

sulfur (10544-50-0) + selenium (7782-49-2) + diphenylphosphane (829-85-6) + sodium hydroxide (1310-73-2) → diphenylthioselenophosphinic acid sodium salt (35351-90-7)

Guidance literature:

In ethanol; at 20 - 50 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/ejic.201200947

Reference yield:

diphenylphosphine selenide (5853-64-5) → diphenylthioselenophosphinic acid sodium salt (35351-90-7)

Guidance literature:

With sulfur; sodium hydroxide; In ethanol; at 23 - 25 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2014.06.013

Reference yield:

diphenylphosphane (829-85-6) → diphenylthioselenophosphinic acid sodium salt (35351-90-7)

Guidance literature:

Multi-step reaction with 2 steps

1: selenium / benzene / 0.5 h / 35 - 40 °C / Inert atmosphere

2: sodium hydroxide; sulfur / ethanol / 0.08 h / 23 - 25 °C / Inert atmosphere

With sulfur; selenium; sodium hydroxide; In ethanol; benzene;

DOI:10.1016/j.jorganchem.2014.06.013

upstream raw materials:

sulfur

selenium

diphenylphosphane

sodium hydroxide

Downstream raw materials:

Se-benzyl diphenylthioselenophosphinate

Se-prop-2-en-1-yl diphenylthioselenophosphinate

nickel(II) diphenylthioselenophosphinate