2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester

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Chemical Name:2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester
CAS No.:869059-97-2
Molecular Formula:C₂₂H₂₆N₂O₃
Molecular Weight:366.46
Hs Code.:

Synonyms:2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester

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Chemical Property of 2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester

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Technology Process of 2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester

There total 2 articles about 2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 64-04-0
phenethylamine

: 144069-67-0,133851-52-2
(S)-N-tert-butoxycarbonylindoline-2-carboxylic acid

: 869059-97-2
2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; In dichloromethane; at 20 ℃; for 16h;

Reference yield: 24.0%

: C₂₂H₂₇BrN₂O₃

: 869059-97-2
2,3-dihydro-2-[[(2-phenylethyl)amino]carbonyl]-(2S)-1H-indole-1-carboxylic acid 1,1-dimethyl ethyl ester

: C₂₂H₂₆N₂O₃

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tert-butylimino-tri(pyrrolidino)phosphorane; XPhos; In 1,4-dioxane; at 65 ℃; for 4h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.02.094