Technology Process of C25H26N4O2
There total 6 articles about C25H26N4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
18-crown-6 ether; potassium tert-butylate;
In
cyclohexane; dimethyl sulfoxide;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.67 h / 80 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere
3.2: 1.83 h / 5 - 20 °C
4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / 100 °C / Inert atmosphere
5.1: potassium tert-butylate; 18-crown-6 ether / dimethyl sulfoxide; cyclohexane / 1 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; potassium tert-butylate; palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate;
In
1,2-dimethoxyethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.67 h / 80 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere
3.2: 1.83 h / 5 - 20 °C
4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / 100 °C / Inert atmosphere
5.1: potassium tert-butylate; 18-crown-6 ether / dimethyl sulfoxide; cyclohexane / 1 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; potassium tert-butylate; palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate;
In
1,2-dimethoxyethane; cyclohexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;