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C13H21Cl2N2O5P

Base Information
  • Chemical Name:C13H21Cl2N2O5P
  • CAS No.:113524-15-5
  • Molecular Formula:C13H21Cl2N2O5P
  • Molecular Weight:387.2
  • Hs Code.:
C<sub>13</sub>H<sub>21</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>5</sub>P

Synonyms:C13H21Cl2N2O5P

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Chemical Property of C13H21Cl2N2O5P
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Technology Process of C13H21Cl2N2O5P

There total 16 articles about C13H21Cl2N2O5P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen; palladium on activated charcoal; In methanol; for 1h; under 760 Torr;
Guidance literature:
Multi-step reaction with 14 steps
1: 62 percent / m-chloroperbenzoic acid / CH2Cl2 / 5 h / 0 °C
2: 85 percent / K2CO3 / butan-2-one / 5 h / Heating
3: 97 percent / N-bromosuccinimide / CCl4 / 1.5 h / Heating; Irradiation
4: 98 percent / aq. AgNO3 / 2-methoxy-ethanol / 0.5 h / Heating
5: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C
6: 84 percent / AlCl3 / chlorobenzene / 0.75 h / Heating
7: 79 percent / HCl / 4 h / Heating
8: 86 percent / K2CO3 / butan-2-one / 16 h / Heating
9: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h
10: 91 percent / NaBH4 / methanol / 1 h / 0 °C
11: 97 percent / pyridine / 16 h
12: 88 percent / SO2Cl2 / diethyl ether / 3 h / Ambient temperature
13: 83 percent / 5 M aq. NaOH / ethanol / 2 h / Heating
14: H2 / 10percent Pd/C / methanol / 1 h / 760 Torr
With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; sulfuryl dichloride; tetra-n-butylammonium permanganate; hexane; hydrogen; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; ethanol; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;
Guidance literature:
Multi-step reaction with 15 steps
1: 86 percent / K2CO3 / butan-2-one / 5 h / Heating
2: 62 percent / m-chloroperbenzoic acid / CH2Cl2 / 5 h / 0 °C
3: 85 percent / K2CO3 / butan-2-one / 5 h / Heating
4: 97 percent / N-bromosuccinimide / CCl4 / 1.5 h / Heating; Irradiation
5: 98 percent / aq. AgNO3 / 2-methoxy-ethanol / 0.5 h / Heating
6: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C
7: 84 percent / AlCl3 / chlorobenzene / 0.75 h / Heating
8: 79 percent / HCl / 4 h / Heating
9: 86 percent / K2CO3 / butan-2-one / 16 h / Heating
10: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h
11: 91 percent / NaBH4 / methanol / 1 h / 0 °C
12: 97 percent / pyridine / 16 h
13: 88 percent / SO2Cl2 / diethyl ether / 3 h / Ambient temperature
14: 83 percent / 5 M aq. NaOH / ethanol / 2 h / Heating
15: H2 / 10percent Pd/C / methanol / 1 h / 760 Torr
With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; sulfuryl dichloride; tetra-n-butylammonium permanganate; hexane; hydrogen; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; ethanol; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;
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