methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

Base Information

Chemical Name:methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate
CAS No.:1286181-00-7
Molecular Formula:C₁₆H₁₃Br₂FO₅S
Molecular Weight:496.149
Hs Code.:

Synonyms:methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

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Chemical Property of methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

Chemical Property:

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Technology Process of methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

There total 4 articles about methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773853-92-2
2-bromo-4-fluorothiophenol

: 1286179-94-9
methyl 3-bromo-6-bromomethyl-2-methoxybenzoate

: 1286181-00-7
methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

Guidance literature:: 2-bromo-4-fluorothiophenol; methyl 3-bromo-6-bromomethyl-2-methoxybenzoate; With potassium carbonate; In tetrahydrofuran; for 1h; Reflux;

With dihydrogen peroxide; In acetic acid; at 20 - 80 ℃; for 2h;

Reference yield:

: methyl 3-bromo-2-methoxy-6-methylbenzoate

: 1286181-00-7
methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 0.67 h / 90 °C

2.1: potassium carbonate / tetrahydrofuran / 1 h / Reflux

2.2: 2 h / 20 - 80 °C

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; potassium carbonate; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 1286179-99-4
methyl 3-bromo-2-hydroxy-6-methylbenzoate

: 1286181-00-7
methyl 3-bromo-6-(2-bromo-4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 2.5 h / Reflux

2.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 0.67 h / 90 °C

3.1: potassium carbonate / tetrahydrofuran / 1 h / Reflux

3.2: 2 h / 20 - 80 °C

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; potassium carbonate; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; 1,2-dichloro-ethane; acetone;