N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

Base Information

Chemical Name:N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide
CAS No.:71956-81-5
Molecular Formula:C₁₈H₂₄N₂O₃
Molecular Weight:316.4
Hs Code.:

Synonyms:N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

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Technology Process of N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

There total 4 articles about N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.3%

: 71956-82-6
N-<2-hydroxy-1-(α-hydroxybenzyl)ethyl>-1-propylnicotinium iodide

: 71956-81-5
N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

Guidance literature:: With sodium dithionite; sodium carbonate; In methanol; chloroform; water; Ambient temperature;

Reference yield:

: 59-67-6
nicotinic acid

: 71956-81-5
N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine, ethyl chloroformate / 1.) toluene, -5 --> -10 deg C, 30 min, 2.) chloroform, room temperature, overnight

2: 47.8 percent / ethanol / 5 h / Heating

3: 81.3 percent / sodium carbonate, sodium dithionite / CHCl₃; methanol; H₂O / Ambient temperature

With sodium dithionite; chloroformic acid ethyl ester; sodium carbonate; triethylamine; In methanol; ethanol; chloroform; water;

Reference yield:

: 74491-53-5
(+)-(4S,5S)-(nicotinoylamino)-2,2-dimethyl-4-phenyl-1,3-dioxan

: 71956-81-5
N-<(1S)-2-hydroxy-1-<(S)-α-hydroxybenzyl>ethyl>-1-propyl-1,4-dihydronicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 47.8 percent / ethanol / 5 h / Heating

2: 81.3 percent / sodium carbonate, sodium dithionite / CHCl₃; methanol; H₂O / Ambient temperature

With sodium dithionite; sodium carbonate; In methanol; ethanol; chloroform; water;