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C14H19NO2Si

Base Information
  • Chemical Name:C14H19NO2Si
  • CAS No.:1089178-87-9
  • Molecular Formula:C14H19NO2Si
  • Molecular Weight:261.396
  • Hs Code.:
C<sub>14</sub>H<sub>19</sub>NO<sub>2</sub>Si

Synonyms:C14H19NO2Si

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Chemical Property of C14H19NO2Si
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Technology Process of C14H19NO2Si

There total 1 articles about C14H19NO2Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C13H18BrNOSi; With isopropylmagnesium chloride; In tetrahydrofuran; n-heptane; toluene; at -50 - -20 ℃; for 1.83333h;
N,N-dimethyl-formamide; In tetrahydrofuran; n-heptane; toluene; at -10 - 20 ℃;
Guidance literature:
ethylene glycol diacetate; C14H19NO2Si; ethylene glycol; With toluene-4-sulfonic acid; In tetrahydrofuran; n-heptane; tert-butyl methyl ether; toluene; at 80 - 95 ℃;
In n-heptane; toluene; at 100 ℃; Dean-Stark trap;
Guidance literature:
Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid / n-heptane; toluene / 100 °C / Heating / reflux
2.1: sodium hydroxide; water / 1,2-dimethoxyethane; toluene / 0.5 h / -20 - 25 °C
2.2: 0 °C / pH 6 - 7
With sodium hydroxide; water; toluene-4-sulfonic acid; In 1,2-dimethoxyethane; n-heptane; toluene;
upstream raw materials:

C13H18BrNOSi

N,N-dimethyl-formamide

Downstream raw materials:

C16H23NO3Si

C10H9NO3

C15H9BrFNO3

C15H9BrF3NO2

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