N,N-Dimethylformamide-15N

Base Information

• Chemical Name: N,N-Dimethylformamide-15N
• CAS No.: 1449-84-9
• Molecular Formula: C₃H₇NO
• Molecular Weight: 74.088
• European Community (EC) Number: 687-098-4
• DSSTox Substance ID: DTXSID40584056
• Nikkaji Number: J1.387.679G
• Wikidata: Q82475686
• Mol file: 1449-84-9.mol

Synonyms:N,N-Dimethylformamide-15N;1449-84-9;N,N-Dimethyl(~15~N)formamide;DTXSID40584056;ZMXDDKWLCZADIW-AZXPZELESA-N;AKOS015913374;N,N-Dimethylformamide-15N,99 atom % 15n;N,N-Dimethylformamide-15N, 98 atom % 15N;J-008035

Chemical Property of N,N-Dimethylformamide-15N

Chemical Property:

• Melting Point: −61 °C(lit.)
• Refractive Index: n20/D 1.431(lit.)
• Boiling Point: 153 °C(lit.)
• Flash Point: 136 °F
• PSA: 20.31000
• Density: 0.957 g/mL at 25 °C
• LogP: 0.34030
• XLogP3: -1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 74.049798741
• Heavy Atom Count: 5
• Complexity: 33.9

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N-Dimethylformamide-15N 98 atom % 15N ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 61-20/21-36
• Safety Statements: 53-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C=O
• Isomeric SMILES: C[15N](C)C=O

Technology Process of N,N-Dimethylformamide-15N

There total 1 articles about N,N-Dimethylformamide-15N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium formate (590-29-4) + 15N-dimethylamine hydrochloride (75693-94-6) → (15)N,(15)N-dimethylformamide (1449-84-9)

Guidance literature:

Yield given; Heating;

Reference yield: 8.0%

N-methyl-2-(4-methoxyphenyl)indole (61843-43-4) + (15)N,(15)N-dimethylformamide (1449-84-9) → C17H14N(15)NO (1354800-17-1)

Guidance literature:

With tetrabutylammomium bromide; copper diacetate; palladium diacetate; potassium carbonate; for 24h;

DOI:10.1021/ja204063z

upstream raw materials:

potassium formate

¹⁵N-dimethylamine hydrochloride

Downstream raw materials:

C₁₇H₁₄N⁽¹⁵⁾NO