1S,2S-N,N'-bis((2,4,6-triMethylphenyl)Methyl)-1,2-diphenyl-1,2-EthanediaMine

Base Information

• Chemical Name: 1S,2S-N,N'-bis((2,4,6-triMethylphenyl)Methyl)-1,2-diphenyl-1,2-EthanediaMine
• CAS No.: 124070-54-8
• Molecular Formula: C₃₄H₄₀N₂
• Molecular Weight: 476.705
• Mol file: 124070-54-8.mol

Synonyms:(1S,2S)-1,2-diphenyl-N¹,N²-bis(mesitylmethyl)ethane-1,2-diamine

Chemical Property of 1S,2S-N,N'-bis((2,4,6-triMethylphenyl)Methyl)-1,2-diphenyl-1,2-EthanediaMine

Chemical Property:

Purity/Quality:

>95%,>98%e.e. ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1S,2S-N,N'-bis((2,4,6-triMethylphenyl)Methyl)-1,2-diphenyl-1,2-EthanediaMine

There total 6 articles about 1S,2S-N,N'-bis((2,4,6-triMethylphenyl)Methyl)-1,2-diphenyl-1,2-EthanediaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.6%

(1S,2S)-(-)-1,2-di(2,4,6-trimethylbenzylideneamino)-1,2-diphenylethane → (1S,2S)-1,2-diphenyl-N1,N2-bis(mesitylmethyl)ethane-1,2-diamine (124070-54-8,138608-02-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol;

DOI:10.1039/b605912k

Reference yield:

(1S,2S)-1,2-Diphenyl-N,N'-bis-[1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-ethane-1,2-diamine (124151-16-2) → (1S,2S)-1,2-diphenyl-N1,N2-bis(mesitylmethyl)ethane-1,2-diamine (124070-54-8,138608-02-3)

Guidance literature:

With sodium tetrahydroborate; In methanol; toluene; Yield given;

DOI:10.1021/ja00208a025

Reference yield:

mesytaldehyde (487-68-3) → (1S,2S)-1,2-diphenyl-N1,N2-bis(mesitylmethyl)ethane-1,2-diamine (124070-54-8,138608-02-3)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 60 °C

2: NaBH₄ / toluene; methanol

With sodium tetrahydroborate; In methanol; toluene;

DOI:10.1021/ja00208a025

upstream raw materials:

(1S,2S)-1,2-Diphenyl-N,N'-bis-[1-(2,4,6-trimethyl-phenyl)-meth-(Z)-ylidene]-ethane-1,2-diamine

mesytaldehyde

(S,S)-1,2-diphenyl-1,2-diaminoethane

Downstream raw materials:

(4S,5S)-1,3-bis(2,4,6-trimethylbenzyl)-4,5-diphenyl-4,5-dihydro-1H-imidazol-3-ium chloride