Technology Process of C17H21F2NO5
There total 6 articles about C17H21F2NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
20 % Pd(OH)2/C; hydrogen; triethylamine;
In
ethanol;
at 22 ℃;
for 2h;
under 10343.2 Torr;
DOI:10.1016/j.bmcl.2011.05.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / tetrahydrofuran / 0.5 h / 22 °C
2: potassium tert-butylate / tetrahydrofuran / 30 °C
3: dihydrogen peroxide; lithium hydroxide / water; dimethyl sulfoxide / 45 °C
4: ethanol; potassium hydroxide / 10 h / 80 °C
5: 20 % Pd(OH)2/C; hydrogen; triethylamine / ethanol / 2 h / 22 °C / 10343.2 Torr
With
ethanol; 20 % Pd(OH)2/C; potassium tert-butylate; hydrogen; dihydrogen peroxide; triethylamine; potassium hydroxide; lithium hydroxide;
In
tetrahydrofuran; ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2011.05.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dihydrogen peroxide; lithium hydroxide / water; dimethyl sulfoxide / 45 °C
2: ethanol; potassium hydroxide / 10 h / 80 °C
3: 20 % Pd(OH)2/C; hydrogen; triethylamine / ethanol / 2 h / 22 °C / 10343.2 Torr
With
ethanol; 20 % Pd(OH)2/C; hydrogen; dihydrogen peroxide; triethylamine; potassium hydroxide; lithium hydroxide;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2011.05.014