(S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

Base Information

Chemical Name:(S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester
CAS No.:126110-96-1
Molecular Formula:C₃₇H₄₀N₂O₈
Molecular Weight:640.733
Hs Code.:

Synonyms:(S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

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Chemical Property of (S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

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Technology Process of (S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

There total 5 articles about (S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126132-92-1
<(3,4-dimethoxyphenyl)amino>acetic acid methyl ester

: 126110-96-1
(S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) pyridine / tetrahydrofuran / 1.) room temp., 16 h, 2.) room temp., 24 h

2: 1 N LiOH / dioxane / 1 h / Ambient temperature

3: ethyl acetate / 48 h / Ambient temperature

With pyridine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethyl acetate;
DOI:10.1021/jm00167a028

Reference yield:

: 59221-35-1
(S)-6-[[(Phenylmethoxy)carbonyl]amino]-2-hydroxyhexanoic acid

: 126110-96-1
(S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / triethylamine / tetrahydrofuran / 2 h / 0 °C

2: Et₃N, 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 0 °C

3: 2.) pyridine / tetrahydrofuran / 1.) room temp., 16 h, 2.) room temp., 24 h

4: 1 N LiOH / dioxane / 1 h / Ambient temperature

5: ethyl acetate / 48 h / Ambient temperature

With pyridine; dmap; lithium hydroxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethyl acetate;
DOI:10.1021/jm00167a028

Reference yield:

: 126111-17-9
(S)-2-(acetyloxy)-6-<<(phenylmethoxy)carbonyl>amino>hexanoic acid

: 126110-96-1
(S)-<<2-hydroxy-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>(2,3-dimethoxyphenyl)amino>acetic acid diphenylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N, 4-(dimethylamino)pyridine / tetrahydrofuran / 2 h / 0 °C

2: 2.) pyridine / tetrahydrofuran / 1.) room temp., 16 h, 2.) room temp., 24 h

3: 1 N LiOH / dioxane / 1 h / Ambient temperature

4: ethyl acetate / 48 h / Ambient temperature

With pyridine; dmap; lithium hydroxide; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethyl acetate;
DOI:10.1021/jm00167a028