benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

Base Information

Chemical Name:benzyl 2-[trans-4-(amino)-cyclohexyl]acetate
CAS No.:1374760-13-0
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:

Synonyms:benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

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Chemical Property of benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

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Technology Process of benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

There total 3 articles about benzyl 2-[trans-4-(amino)-cyclohexyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374760-11-8
C₂₀H₂₉NO₄

: 1374760-13-0
benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

Guidance literature:: C₂₀H₂₉NO₄; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;

In methanol; at 0 ℃; pH=7.5;

Reference yield:

: 2-(4-((tert-butoxycarbonyl)amino)cyclohexyl)acetic acid

: 100-39-0
benzyl bromide

: 1374760-13-0
benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

Guidance literature:: 2-(4-((tert-butoxycarbonyl)amino)cyclohexyl)acetic acid; benzyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; for 16.75h;

With trifluoroacetic acid; In dichloromethane; for 2.5h;

Reference yield:

: 100-39-0
benzyl bromide

: 1374760-13-0
benzyl 2-[trans-4-(amino)-cyclohexyl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

2.2: Dowex Monosphere (OH^(1-)) (550 A) / 0 °C / pH 7.5

With caesium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;