C₁₃H₁₆O₄

Base Information

Chemical Name:C₁₃H₁₆O₄
CAS No.:36440-86-5
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

C<sub>13</sub>H<sub>16</sub>O<sub>4</sub>

Synonyms:C₁₃H₁₆O₄

Suppliers and Price of C₁₃H₁₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₆O₄

Chemical Property:

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Technology Process of C₁₃H₁₆O₄

There total 4 articles about C₁₃H₁₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 887339-22-2
ethyl 4-((1E)-3-carboxyprop-1-enyl)benzoate

: 36440-86-5
C₁₃H₁₆O₄

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃; for 3h;

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1253596-90-5
C₂₀H₂₉BO₂

: 36440-86-5
C₁₃H₁₆O₄

Guidance literature:: carbon dioxide; C₂₀H₂₉BO₂; With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); lithium methanolate; In tetrahydrofuran; at 70 ℃; for 24h; under 760.051 Torr; Inert atmosphere;

With hydrogenchloride; In water; Inert atmosphere;
DOI:10.1002/anie.201101769

Reference yield:

: 5798-75-4
Ethyl 4-bromobenzoate

: 36440-86-5
C₁₃H₁₆O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); lithium methanolate / tetrahydrofuran / 24 h / 70 °C / 760.05 Torr / Inert atmosphere

3.2: Inert atmosphere

With n-butyllithium; chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); lithium methanolate; In tetrahydrofuran; hexane;
DOI:10.1002/anie.201101769