2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole

Base Information

• Chemical Name: 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole
• CAS No.: 42017-10-7
• Molecular Formula: C₁₉H₂₉BO
• Molecular Weight: 284.25
• Mol file: 42017-10-7.mol

Synonyms:2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole

Chemical Property of 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole

There total 4 articles about 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

K(1+)*{(C3H7)3BCCC6H5}(1-)=K{(C3H7)3BCCC6H5} + acetyl chloride (75-36-5) → 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole (42017-10-7) + 4-phenyl-3-butyne-2-one (1817-57-8)

Guidance literature:

DOI:10.1016/S0040-4039(01)95715-6

Reference yield:

Li(1+)*{(C3H7)3BCCC6H5}(1-)=Li{(C3H7)3BCCC6H5} (74858-62-1) + acetyl chloride (75-36-5) → 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole (42017-10-7) + 4-phenyl-3-butyne-2-one (1817-57-8)

Guidance literature:

DOI:10.1016/S0040-4039(01)95715-6

Reference yield:

Natrium-(tripropyl-phenylethinyl-boranat) (14839-41-9) + acetyl chloride (75-36-5) → 2,3,3-triisopropyl-5-methyl-4-phenyl-2,3-dihydro-[1,2]oxaborole (42017-10-7) + 4-phenyl-3-butyne-2-one (1817-57-8)

Guidance literature:

DOI:10.1016/S0040-4039(01)95715-6

upstream raw materials:

acetyl chloride

Li⁽¹⁺⁾*{(C₃H₇)3BCCC₆H₅}^(1-)=Li{(C₃H₇)3BCCC₆H₅}

Natrium-(tripropyl-phenylethinyl-boranat)