4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

Base Information

Chemical Name:4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine
CAS No.:1404222-74-7
Molecular Formula:C₆₂H₄₂N₂
Molecular Weight:815.029
Hs Code.:

Synonyms:4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

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Chemical Property of 4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

Chemical Property:

Purity/Quality:

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Technology Process of 4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

There total 10 articles about 4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 331980-55-3
4'-(carbazol-9-yl)-N-phenyl-[1,1'-biphenyl]-4-amine

: 1123921-68-5
2-(4-bromophenyl)-9,10-diphenylanthracene

: 1404222-74-7
4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

Guidance literature:: With tri-tert-butyl phosphine; sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In hexane; toluene; at 80 ℃; for 3h; Inert atmosphere;

Reference yield:

: 572-83-8
2-bromoanthracene-9,10-dione

: 1404222-74-7
4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2.1: potassium iodide; acetic acid; sodium hypophosphite monohydrate / 2 h / 120 °C

2.2: 1 h / 120 °C

3.1: n-butyllithium; sodium thiosulfate / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 13 h / -78 - 20 °C

3.3: 1 h / 20 °C

4.1: potassium carbonate; tris-(o-tolyl)phosphine / palladium diacetate / toluene; ethanol; water / 8 h / 100 °C / Inert atmosphere

5.1: sodium t-butanolate; tri-tert-butyl phosphine / bis(dibenzylideneacetone)-palladium⁽⁰⁾ / toluene; hexane / 3 h / 80 °C / Inert atmosphere

With n-butyllithium; sodium hypophosphite monohydrate; tri-tert-butyl phosphine; potassium carbonate; sodium thiosulfate; acetic acid; tris-(o-tolyl)phosphine; potassium iodide; sodium t-butanolate; palladium diacetate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; water; toluene;

Reference yield:

: 419536-33-7
4-(carbazol-9-yl)phenylboronic acid

: 54446-36-5
4-bromodiphenylamine

: 1404222-74-7
4-[4-(9H-carbazol-9-yl)phenyl]-4'-(9,10-diphenyl-2-anthryl)triphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: tri-tert-butyl phosphine / palladium diacetate / toluene; ethanol; water / 6.5 h / 100 °C / Inert atmosphere

2: sodium t-butanolate; tri-tert-butyl phosphine / bis(dibenzylideneacetone)-palladium⁽⁰⁾ / toluene; hexane / 3 h / 80 °C / Inert atmosphere

With tri-tert-butyl phosphine; sodium t-butanolate; palladium diacetate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In ethanol; hexane; water; toluene;