3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

Base Information

Chemical Name:3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide
CAS No.:152945-53-4
Molecular Formula:C₁₈H₁₇ClN₂O₃
Molecular Weight:344.798
Hs Code.:

Synonyms:3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

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Technology Process of 3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

There total 4 articles about 3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3-(4-Chloro-phenyl)-4-cyano-5-hydroxy-furan-2-carboxylic acid cyclohexylamide; compound with piperidine

: 152945-53-4
3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

Guidance literature:: With hydrogenchloride; In methanol; at 5 ℃;
DOI:10.1055/s-1993-25940

Reference yield:

: 152945-46-5
Cyano-acetic acid 2-(4-chloro-phenyl)-1-cyclohexylcarbamoyl-2-oxo-ethyl ester

: 152945-53-4
3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

Guidance literature:: With hydrogenchloride; triethylamine; Yield given. Multistep reaction; 1.) MeOH, room temp., 10 min, 2.) MeOH, 5 deg C, pH=4;
DOI:10.1055/s-1993-25940

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 152945-53-4
3-(4-Chloro-phenyl)-4-cyano-5-oxo-2,5-dihydro-furan-2-carboxylic acid cyclohexylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / diethyl ether / 6 h / Ambient temperature

2: 63 percent / methanol / Ambient temperature

3: 100 percent / 6N HCl / methanol / 5 °C

With hydrogenchloride; In methanol; diethyl ether;
DOI:10.1055/s-1993-25940