(S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

Base Information

Chemical Name:(S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride
CAS No.:1264239-91-9
Molecular Formula:C₁₇H₂₄N₂O₄*ClH
Molecular Weight:356.849
Hs Code.:

Synonyms:(S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

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Chemical Property of (S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

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Technology Process of (S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

There total 8 articles about (S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1264239-87-3
C₁₉H₂₃F₃N₂O₅

: 1264239-91-9
(S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

Guidance literature:: C₁₉H₂₃F₃N₂O₅; With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;

With water; lithium hydroxide; In tetrahydrofuran;

With thionyl chloride; allyl alcohol; at 20 - 70 ℃; for 19h;

Reference yield: 83.0%

: 107-18-6
allyl alcohol

: N^α-Benzyloxycarbonyl-N^δ-methyl-L-ornithin

: 1264239-91-9
(S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

Guidance literature:: With thionyl chloride; at 20 - 70 ℃; for 2h;

Reference yield:

: 2640-58-6
Nα-benzyloxycarbonyl-L-ornithine

: 1264239-91-9
(S)-allyl 2-(benzyloxycarbonylamino)-5-(methylamino)pentanoate hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / benzene

2: triethylamine / dichloromethane; methanol

3: potassium carbonate / N,N-dimethyl-formamide / 8 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran

5: lithium hydroxide monohydrate / water; tetrahydrofuran

6: thionyl chloride / 2 h / 20 - 70 °C

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; lithium hydroxide monohydrate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;