propyl (2-phenylethynyl) sulfide

Base Information

Chemical Name:propyl (2-phenylethynyl) sulfide
CAS No.:1355700-52-5
Molecular Formula:C₁₁H₁₂S
Molecular Weight:176.282
Hs Code.:

Synonyms:propyl (2-phenylethynyl) sulfide

Suppliers and Price of propyl (2-phenylethynyl) sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propyl (2-phenylethynyl) sulfide

Chemical Property:

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Technology Process of propyl (2-phenylethynyl) sulfide

There total 3 articles about propyl (2-phenylethynyl) sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 106-94-5
propyl bromide

: 536-74-3
phenylacetylene

: 1355700-52-5
propyl (2-phenylethynyl) sulfide

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With sulfur; In tetrahydrofuran; hexane; at -78 - 0 ℃; Inert atmosphere;

propyl bromide; Further stages;
DOI:10.1002/hc.20744

Reference yield:

: 20568-13-2
lithium 2-phenylethynethiolate

: 1355700-52-5
propyl (2-phenylethynyl) sulfide

Guidance literature:: In tetrahydrofuran; hexane; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b03590

Reference yield:

: 536-74-3
phenylacetylene

: 629-19-6
Dipropyl disulfide

: 1355700-52-5
propyl (2-phenylethynyl) sulfide

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

Dipropyl disulfide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1039/d1cc02249k