Ethynethiol, phenyl-, lithium salt

Base Information

Chemical Name:Ethynethiol, phenyl-, lithium salt
CAS No.:20568-13-2
Molecular Formula:C8H6S.Li
Molecular Weight:140.135
Hs Code.:

Synonyms:lithium ethyne-thiolate;LiSCCPh;lithium phenylethynethiolate;phenyl-ethynethiolate;Lithium;

Suppliers and Price of Ethynethiol, phenyl-, lithium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethynethiol, phenyl-, lithium salt

Chemical Property:

PSA：0.00000
LogP:1.54250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethynethiol, phenyl-, lithium salt

There total 2 articles about Ethynethiol, phenyl-, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 536-74-3
phenylacetylene

: 20568-13-2
lithium 2-phenylethynethiolate

Guidance literature:: phenylacetylene; With n-butyllithium; In hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With sulfur; In hexane; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201101948

Reference yield: 70.0%

: 25445-77-6
4-phenyl-1,2,3-thiadiazole

: 20568-13-2
lithium 2-phenylethynethiolate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; diethyl ether; for 0.5h;

Reference yield: 89.0%

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 20568-13-2
lithium 2-phenylethynethiolate

: (η5-cyclopentadienyl)ruthenium(II)(PPh3)2(SCCPh)

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; mixt. of Ru complex, PPh3 and excess of LiSCCPh is heated under reflux (N2, THF, 30 min); evapn., addn. of benzene, filtn. (Celite), concn. and hexane/Et2O is added, filtn., ppt. is washed with hexane, dried in vac., elem. anal.;