1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

Base Information

Chemical Name:1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone
CAS No.:115262-72-1
Molecular Formula:C₂₅H₂₇NO₅
Molecular Weight:421.493
Hs Code.:

Synonyms:1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

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Chemical Property of 1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

Chemical Property:

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Technology Process of 1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

There total 8 articles about 1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115262-40-3
1-(4-benzyloxy-3-methoxyphenethyl)-3-(1,1-ethylenedioxyethyl)pyridinium bromide

: 115262-72-1
1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

Guidance literature:: With potassium hydroxide; potassium hexacyanoferrate(III); In water; benzene; at 32 ℃; for 5h; Yield given;

Reference yield:

: 55676-25-0
3-(2-methyl-[1,3]dioxolan-2-yl)-pyridine

: 115262-72-1
1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

Guidance literature:: Multi-step reaction with 2 steps

1: 13.2 g / benzene / 72 h / Heating

2: K₃Fe(CN)6, KOH / H₂O; benzene / 5 h / 32 °C

With potassium hydroxide; potassium hexacyanoferrate(III); In water; benzene;

Reference yield:

: 1835-11-6
4-benzyloxy-3-methoxyacetophenone

: 115262-72-1
1-(4-benzyloxy-3-methoxyphenethyl)-5-(1,1-ethylenedioxyethyl)-2-(1H)-pyridinone

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) 80 deg C, 1 h; 2.) reflux, 5 h

2: 16.4 g / aq. KOH (50percent) / ethanol / 5 h / Heating

3: 94 percent / HCl / 24 h / Ambient temperature

4: 96 percent / LiAlH₄ / diethyl ether / 2 h / 0 - 20 °C

5: 92 percent / N-bromosuccinimide, triphenylphosphine (Ph₃P) / benzene / 5 h / 10 - 20 °C

6: 13.2 g / benzene / 72 h / Heating

7: K₃Fe(CN)6, KOH / H₂O; benzene / 5 h / 32 °C

With hydrogenchloride; potassium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; triphenylphosphine; potassium hexacyanoferrate(III); In diethyl ether; ethanol; water; benzene;