C₁₂H₈N₄

Base Information

Chemical Name:C₁₂H₈N₄
CAS No.:1367528-40-2
Molecular Formula:C₁₂H₈N₄
Molecular Weight:208.222
Hs Code.:

C<sub>12</sub>H<sub>8</sub>N<sub>4</sub>

Synonyms:C₁₂H₈N₄

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Chemical Property of C₁₂H₈N₄

Chemical Property:

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Technology Process of C₁₂H₈N₄

There total 6 articles about C₁₂H₈N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 132464-89-2
1-(4-iodo-phenyl)-1H-imidazole

: 109-77-3
malononitrile

: 1367528-40-2
C₁₂H₈N₄

Guidance literature:: malononitrile; With sodium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 1h; Inert atmosphere;

1-(4-iodo-phenyl)-1H-imidazole; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; for 5h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; pH=7; Inert atmosphere;

Reference yield: 87.0%

: 10040-96-7
1-(4-bromophenyl)-1H-imidazole

: 109-77-3
malononitrile

: 1367528-40-2
C₁₂H₈N₄

Guidance literature:: malononitrile; With sodium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 1h; Inert atmosphere;

1-(4-bromophenyl)-1H-imidazole; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; for 5h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; pH=7; Inert atmosphere;

Reference yield:

: C₈H₆BrNO

: 1367528-40-2
C₁₂H₈N₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium chloride / methanol; water / 1 h / Reflux

2.1: sodium hydride / 1,2-dimethoxyethane / 1 h / 20 °C / Inert atmosphere

2.2: 5 h / Inert atmosphere; Reflux

2.3: pH 7 / Inert atmosphere

With sodium hydride; ammonium chloride; In methanol; 1,2-dimethoxyethane; water;