methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate

Base Information

Chemical Name:methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate
CAS No.:81109-94-6
Molecular Formula:C₂HF₃O₂*C₁₃H₁₈N₂O₃
Molecular Weight:364.321
Hs Code.:

Synonyms:methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate

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Chemical Property of methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate

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Technology Process of methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate

There total 3 articles about methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 15136-29-5
(S)-methyl 2-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)propanoate

: 76-05-1
trifluoroacetic acid

: 81109-94-6
methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate

Guidance literature:: In dichloromethane;
DOI:10.1016/S0040-4020(01)88529-X

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 81109-94-6
methyl (2S)‐2‐[(2S)‐2‐amino‐3‐phenylpropanamido]propanoate trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

2: 100 percent / CH₂Cl₂

In dichloromethane;
DOI:10.1016/S0040-4020(01)88529-X

Reference yield:

: 18942-49-9
Boc-D-Phe-OH

: 81109-94-6
(S)-2-((R)-2-Amino-3-phenyl-propionylamino)-propionic acid methyl ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: BOP, triethylamine / acetonitrile / 2 h

2: methylene chloride / 0.5 h

With dichloromethane; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In acetonitrile;
DOI:10.1016/0040-4020(81)85016-8