(R)-1-(3-formylphenyl)octyl acetate

Base Information

Chemical Name:(R)-1-(3-formylphenyl)octyl acetate
CAS No.:1372526-65-2
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:(R)-1-(3-formylphenyl)octyl acetate

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Chemical Property of (R)-1-(3-formylphenyl)octyl acetate

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Technology Process of (R)-1-(3-formylphenyl)octyl acetate

There total 5 articles about (R)-1-(3-formylphenyl)octyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372526-63-0
(R)-1-(3-(hydroxymethyl)phenyl)octyl acetate

: 1372526-65-2
(R)-1-(3-formylphenyl)octyl acetate

Guidance literature:: (R)-1-(3-(hydroxymethyl)phenyl)octyl acetate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.5h;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1021/jm201608g

Reference yield:

: 1372526-64-1
(R)-1-(3-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)octyl acetate

: 1372526-65-2
(R)-1-(3-formylphenyl)octyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

2.2: 1 h / -78 - 20 °C

With oxalyl dichloride; tetrabutyl ammonium fluoride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1021/jm201608g

Reference yield:

: 200886-71-1
N-methoxy-N-methyloctanamide

: 1372526-65-2
(R)-1-(3-formylphenyl)octyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 2.5 h / 0 °C

1.2: 3 h / -78 - 0 °C

2.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / -78 - -15 °C

3.1: pyridine / 5 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

5.2: 1 h / -78 - 20 °C

With pyridine; oxalyl dichloride; tetrabutyl ammonium fluoride; isopropylmagnesium chloride; dimethyl sulfoxide; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; 1.1: Grignard reaction / 1.2: Grignard reaction / 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.1021/jm201608g