C₁₃H₁₃F₃O₇S

Base Information

• Chemical Name: C₁₃H₁₃F₃O₇S
• CAS No.: 431049-88-6
• Molecular Formula: C₁₃H₁₃F₃O₇S
• Molecular Weight: 370.303
• Mol file: 431049-88-6.mol

Synonyms:C₁₃H₁₃F₃O₇S

Chemical Property of C₁₃H₁₃F₃O₇S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₃F₃O₇S

There total 3 articles about C₁₃H₁₃F₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C13H13F3O6S (431049-87-5) → C13H13F3O7S (431049-88-6)

Guidance literature:

With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; In water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2013.06.028

Reference yield:

2-hydroxy-5-formylbenzoic acid (616-76-2) → C13H13F3O7S (431049-88-6)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran

2: pyridine / -10 °C

3: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water

With pyridine; dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2013.06.028

Reference yield:

tert-butyl 5-formyl-2-hydroxybenzoate (431049-86-4) → C13H13F3O7S (431049-88-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / -10 °C

2: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water

With pyridine; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; In water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2013.06.028

upstream raw materials:

2-hydroxy-5-formylbenzoic acid

tert-butyl 5-formyl-2-hydroxybenzoate

C₁₃H₁₃F₃O₆S

Downstream raw materials:

C₁₈H₂₄F₃NO₆S

C₂₅H₄₀F₃NO₇SSi

C₂₉H₂₉N₅O₅

C₃₀H₃₁N₅O₆