(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

Base Information

Chemical Name:(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester
CAS No.:955406-23-2
Molecular Formula:C₂₀H₁₇Cl₂F₆N₃O₆S₂
Molecular Weight:644.4
Hs Code.:

(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

Synonyms:(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

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Chemical Property of (3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

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Technology Process of (3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

There total 9 articles about (3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 955406-15-2
(3R,5S)-3-(4-hydroxy-2,6-dichloro-benzyl)-1-(4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-2-one

: 955406-23-2
(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

: 955407-58-6
C₂₀H₁₇Cl₂F₆N₃O₆S₂

Guidance literature:: With pyridine; at 0 - 20 ℃; for 4.01h;

Reference yield:

: 955373-73-6
(R)-4-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-3-(4-benzyloxy-2,6-dichloro-benzyl)-4-oxo-butyraldehyde

: 955406-23-2
(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

: 955407-58-6
C₂₀H₁₇Cl₂F₆N₃O₆S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,2-dichloro-ethane; isopropyl alcohol / 17 h / 20 °C

1.2: 2 h / 20 °C

1.3: 1 h / 20 °C

2.1: hydrogen / palladium dihydroxide / ethanol / 6 h / 1551.49 Torr

3.1: pyridine / 4.01 h / 0 - 20 °C

With pyridine; hydrogen; palladium dihydroxide; In ethanol; 1,2-dichloro-ethane; isopropyl alcohol;

Reference yield:

: 955373-72-5
(R)-4-benzyl-3-[(S)-2-(4-benzyloxy-2,6-dichloro-benzyl)-pent-4-enoyl]-oxazolidin-2-onecf

: 955406-23-2
(3R,5R)-trifluoro-methanesulfonic acid 3,5-dichloro-4-[2-oxo-1-(2-trifluoromethanesulfonyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)-pyrrolidin-3-ylmethyl]-phenyl ester

: 955407-58-6
C₂₀H₁₇Cl₂F₆N₃O₆S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate / osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 4 h / 20 °C

2.1: 1,2-dichloro-ethane; isopropyl alcohol / 17 h / 20 °C

2.2: 2 h / 20 °C

2.3: 1 h / 20 °C

3.1: hydrogen / palladium dihydroxide / ethanol / 6 h / 1551.49 Torr

4.1: pyridine / 4.01 h / 0 - 20 °C

With pyridine; sodium periodate; hydrogen; palladium dihydroxide; osmium(VIII) oxide; In tetrahydrofuran; ethanol; water; 1,2-dichloro-ethane; isopropyl alcohol; tert-butyl alcohol;