permethylscandocene hydride

Base Information

• Chemical Name: permethylscandocene hydride
• CAS No.: 117024-45-0
• Molecular Formula: C₂₀H₃₁Sc
• Molecular Weight: 316.422

Synonyms:permethylscandocene hydride

Chemical Property of permethylscandocene hydride

Chemical Property:

Purity/Quality:

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Technology Process of permethylscandocene hydride

There total 14 articles about permethylscandocene hydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

(C5(CH3)5)2Sc(SiH2Si(C6H5)3) (842173-44-8) + benzene-d6 (1076-43-3) → permethylscandocene hydride (117024-45-0) + (C5(CH3)5)2Sc(C6(2)H5) (105564-10-1) + (C5(CH3)5)2Sc(SiH(2)HSi(C6H5)3) (842173-49-3) + (C5(CH3)5)2Sc(Si(2)H2Si(C6H5)3) (842173-50-6)

Guidance literature:

In benzene-d6; under Ar; benzene-d6 soln. of Sc complex heated at 65°C for 24 h; not isolated; detd. by (1)H NMR spectra; Kinetics;

DOI:10.1021/ja040141r

Reference yield:

(CpMe5)2ScCH2CH2C6H5 (117024-43-8) → styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + permethylscandocene hydride (117024-45-0)

Guidance literature:

In ⁽²⁾H₈-toluene; sealed NMR tube, 280 K; in several cases in presence of 2-butyne; monitoring reaction by NMR; Kinetics;

Reference yield:

(C5(CH3)5)2ScCH2CH2C6H4N(CH3)2 → permethylscandocene hydride (117024-45-0) + N,N-dimethy-4-vinylaniline (2039-80-7)

Guidance literature:

In ⁽²⁾H₈-toluene; sealed NMR tube, 280 K; monitoring reaction by NMR; Kinetics;

upstream raw materials:

(CpMe₅)2ScCH₂CH₂C₆H₅

(C₅(CH₃)5)2Sc(C₆H₅)

benzene-d6

phenylsilane

Downstream raw materials:

(C₅(CH₃)5)2Sc(C₆H₅)

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