chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene

Base Information

Chemical Name:chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene
CAS No.:748817-36-9
Molecular Formula:C₃₂H₃₁ClS₅Ti
Molecular Weight:659.261
Hs Code.:

Synonyms:chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene

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Technology Process of chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene

There total 1 articles about chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 88510-18-3
1,4-{(C₅H₅)2Ti}S₄C(CH₃)2

: 24165-03-5
tritylsulfenyl chloride

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 748817-36-9
chloro(3,3-dimethyl-7,7,7-triphenyl-1,2,4,5,6-pentathiaheptyl)titanocene

Guidance literature:: In benzene; (exclusion of moisture), ligand and Ti complex stirred in benzene at 30-40°C for 150 min; evapd.(vac.), dissolved (CS2), treated with n-pentane, cooled to -26°C, isolated, washed (n-pentane), dried (air), elem. anal.;
DOI:10.1002/ejic.200300591