Technology Process of C29H39N7O4
There total 10 articles about C29H39N7O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane; chlorotriisopropylsilane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: acetic acid / 1,2-dichloro-ethane
2.1: sodium triacetoxy borohydride / 1,2-dichloro-ethane / 5 h / 20 °C
3.1: methanol
4.1: methanol
5.1: sodium cyanoborohydride / methanol / 6 h
6.1: toluene-4-sulfonic acid / 1,4-dioxane; isopropyl alcohol / 120 h / 80 °C
6.2: 6 h / 20 °C
7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 1 h / 20 °C
8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 - 70 °C
9.1: trifluoroacetic acid / dichloromethane; chlorotriisopropylsilane / 20 °C
With
sodium triacetoxy borohydride; sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; methanol; dichloromethane; chlorotriisopropylsilane; 1,2-dichloro-ethane; isopropyl alcohol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: acetic acid / 1,2-dichloro-ethane
2.1: acetic acid / 1,2-dichloro-ethane
3.1: sodium triacetoxy borohydride / 1,2-dichloro-ethane / 5 h / 20 °C
4.1: methanol
5.1: methanol
6.1: sodium cyanoborohydride / methanol / 6 h
7.1: toluene-4-sulfonic acid / 1,4-dioxane; isopropyl alcohol / 120 h / 80 °C
7.2: 6 h / 20 °C
8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 1 h / 20 °C
9.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 - 70 °C
10.1: trifluoroacetic acid / dichloromethane; chlorotriisopropylsilane / 20 °C
With
sodium triacetoxy borohydride; sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; methanol; dichloromethane; chlorotriisopropylsilane; 1,2-dichloro-ethane; isopropyl alcohol; acetonitrile;