(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

Base Information

Chemical Name:(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone
CAS No.:1007893-80-2
Molecular Formula:C₁₈H₉Br₃N₂O₂
Molecular Weight:524.994
Hs Code.:

Synonyms:(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

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Chemical Property of (7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

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Technology Process of (7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

There total 19 articles about (7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: (3,5-dibromo-4-methoxyphenyl)(7-bromo-9H-pyrido[3,4-b]indol-1-yl)methanone

: 1007893-80-2
(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

Guidance literature:: With hydrogen bromide; In water; acetic acid; at 110 ℃;
DOI:10.1002/ejoc.201300080

Reference yield: 86.0%

: 1435263-19-6
(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(4-hydroxyphenyl)methanone

: 1007893-80-2
(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

Guidance literature:: With phenyltrimethylammonium tribromide; In methanol; dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1039/c3ob40661j

Reference yield:

: 319493-08-8
6-bromo-3-(2-nitroethyl)-1H-indole

: 1007893-80-2
(7-bromo-9H-pyrido[3,4-b]indol-1-yl)(3,5-dibromo-4-hydroxyphenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride; zinc / methanol; water / 3 h / Reflux

2: sodium hydroxide / water; dichloromethane / 1 h / 0 - 10 °C

3: trichlorophosphate / ethyl acetate / 1.5 h / Reflux

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide / 20 °C

5: hydrogen bromide / water; acetic acid / 110 °C

With hydrogenchloride; hydrogen bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; zinc; trichlorophosphate; In methanol; dichloromethane; water; acetic acid; dimethyl sulfoxide; ethyl acetate;
DOI:10.1002/ejoc.201300080