(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

Base Information

Chemical Name:(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride
CAS No.:1393803-00-3
Molecular Formula:C₂₅H₂₆N₃O*Cl
Molecular Weight:419.954
Hs Code.:

Synonyms:(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

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Chemical Property of (S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

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Technology Process of (S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

There total 3 articles about (S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₇N₃O*ClH

: 149-73-5
trimethyl orthoformate

: 1393803-00-3
(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

Guidance literature:: In methanol; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.06.002

Reference yield:

: 3182-95-4
L-Phenylalaninol

: 1393803-00-3
(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

2: ethyl acetate / 2 h / 20 °C / Inert atmosphere

3: dichloromethane / 24 h / 20 °C / Inert atmosphere

4: methanol / 5.5 h / 20 - 50 °C / Inert atmosphere

5: methanol / 24 h / 80 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.tetasy.2012.06.002

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1393803-00-3
(S)-4-(1-(benzyloxy)-3-phenylpropan-2-yl)-3-methyl-1-phenyl-4H-1,2,4-triazol-1-ium chloride

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

2: sodium hydride / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

3: ethyl acetate / 2 h / 20 °C / Inert atmosphere

4: dichloromethane / 24 h / 20 °C / Inert atmosphere

5: methanol / 5.5 h / 20 - 50 °C / Inert atmosphere

6: methanol / 24 h / 80 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.tetasy.2012.06.002