6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide

Base Information

• Chemical Name: 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide
• CAS No.: 78570-32-8
• Molecular Formula: C₁₁H₁₉N₂O*I
• Molecular Weight: 322.189
• Mol file: 78570-32-8.mol

Synonyms:6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide

Chemical Property of 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide

There total 5 articles about 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetone (67-64-1) → 4-methyl-pent-3-en-2-one (141-79-7) + 4-Hydroxy-4-methyl-2-pentanone (123-42-2) + 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide (78570-32-8)

Guidance literature:

for 72h; Heating;

DOI:10.1039/c39810000348

Reference yield:

4-Hydroxy-4-methyl-2-pentanone (123-42-2) → 4-methyl-pent-3-en-2-one (141-79-7) + 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide (78570-32-8) + 2C11H19N2O(1+)*I2*2I(1-)

Guidance literature:

for 48h; Heating;

DOI:10.1039/c39810000348

Reference yield:

(hydridotris(3,5-dimethyl-1-pyrazolyl)borate)nitrosylmolybdenum diiodide → [Mo(tris-(3,5-dimethylpyrazolyl)borate)(NO)(I)]2(μ-O) + {Mo(tris(3,5-dimethylpyrazolyl)borate)(NO)(OEt)I} + 6-hydroxy-2,4-6,8,8-pentamethyl-1,5-diazabicyclo[3.3.0]octa-1,3-dien-1-onium iodide (78570-32-8)

Guidance literature:

With acetone; In acetone; byproducts: mesytyl oxide, isomesytyl oxide, diacetone alcohol; refluxed for 3 d;

DOI:10.1039/c39810000348

upstream raw materials:

4-Hydroxy-4-methyl-2-pentanone

acetone