C₂₈H₄₄O₆

Base Information

Chemical Name:C₂₈H₄₄O₆
CAS No.:1309955-95-0
Molecular Formula:C₂₈H₄₄O₆
Molecular Weight:476.654
Hs Code.:

C<sub>28</sub>H<sub>44</sub>O<sub>6</sub>

Synonyms:C₂₈H₄₄O₆

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Chemical Property of C₂₈H₄₄O₆

Chemical Property:

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Technology Process of C₂₈H₄₄O₆

There total 17 articles about C₂₈H₄₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309956-07-7
C₄₆H₈₄O₆Si₂

: 1309955-95-0
C₂₈H₄₄O₆

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 130 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ol200966z

Reference yield:

: 1309956-02-2
C₂₇H₄₄O₃Si

: 1309955-95-0
C₂₈H₄₄O₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 25 - 60 °C / Inert atmosphere

1.2: 15 h / 25 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere

2.2: 0 - 25 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: sodium hydride / methanol / 0 - 25 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 4 h / 25 °C / Inert atmosphere

8.1: potassium tert-butylate / tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

9.1: ammonia; lithium / tetrahydrofuran; ethanol / -78 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

10.2: 0.5 h / 0 °C / Inert atmosphere

11.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / -78 °C / Inert atmosphere

12.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

12.2: 15 h / 20 °C / Inert atmosphere

13.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Inert atmosphere; Microwave irradiation

With sodium tetrahydroborate; borane-THF; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; lithium; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Hydroboration reaction / 7.1: Michael addition / 8.1: Robinson cyclization;
DOI:10.1021/ol200966z

Reference yield:

: 1309955-89-2
C₂₇H₄₂O₃Si

: 1309955-95-0
C₂₈H₄₄O₆

Guidance literature:: Multi-step reaction with 14 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 25 - 60 °C / Inert atmosphere

2.2: 15 h / 25 °C / Inert atmosphere

3.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere

3.2: 0 - 25 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

7.1: sodium hydride / methanol / 0 - 25 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 4 h / 25 °C / Inert atmosphere

9.1: potassium tert-butylate / tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

10.1: ammonia; lithium / tetrahydrofuran; ethanol / -78 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

11.2: 0.5 h / 0 °C / Inert atmosphere

12.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / -78 °C / Inert atmosphere

13.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

13.2: 15 h / 20 °C / Inert atmosphere

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Inert atmosphere; Microwave irradiation

With sodium tetrahydroborate; borane-THF; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; lithium; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Hydroboration reaction / 8.1: Michael addition / 9.1: Robinson cyclization;
DOI:10.1021/ol200966z