(E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide

Base Information

• Chemical Name: (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide
• CAS No.: 1311378-47-8
• Molecular Formula: C₂₄H₁₈F₃NO₂
• Molecular Weight: 409.408

Synonyms:(E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide

Chemical Property of (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide

Chemical Property:

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Technology Process of (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide

There total 12 articles about (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-4-(trifluoromethyl)benzaldehyde O-[3-(4-methoxyphenyl)-1-phenylprop-2-yn-1-yl]oxime (1311378-34-3) → (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide (1311378-47-8) + (E)-4-(4-methoxyphenyl)-2-phenyl-3-(4-(trifluoromethyl)benzylidene)-2,3-dihydroazete 1-oxide (1311378-48-9)

Guidance literature:

With copper(l) chloride; In toluene; at 100 ℃; for 24h; optical yield given as %de; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol2012583

Reference yield:

(E)-4-(trifluoromethyl)benzaldehyde O-[3-(4-methoxyphenyl)-1-phenylprop-2-yn-1-yl]oxime (1311378-34-3) → (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide (1311378-47-8) + (Z)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide (1311378-60-5) + (E)-4-(4-methoxyphenyl)-2-phenyl-3-(4-(trifluoromethyl)benzylidene)-2,3-dihydroazete 1-oxide (1311378-48-9)

Guidance literature:

With [CuCl(cod)]2; In acetonitrile; at 70 ℃; for 16h; optical yield given as %de; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol2012583

Reference yield:

(Z)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide (1311378-60-5) → (E)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide (1311378-47-8) + (E)-4-(4-methoxyphenyl)-2-phenyl-3-(4-(trifluoromethyl)benzylidene)-2,3-dihydroazete 1-oxide (1311378-48-9)

Guidance literature:

In acetonitrile; at 100 ℃; for 12h; optical yield given as %de; regioselective reaction; Inert atmosphere;

DOI:10.1021/ol2012583

upstream raw materials:

4-(trifluoromethyl)benzaldehyde O-[3-(4-methoxyphenyl)-1-phenylprop-2-yn-1-yl]oxime

(Z)-3-benzylidene-4-(4-methoxyphenyl)-2-(4-(trifluoromethyl)phenyl)-2,3-dihydroazete 1-oxide

(E)-4-(trifluoromethyl)benzaldehyde O-[3-(4-methoxyphenyl)-1-phenylprop-2-yn-1-yl]oxime

4-Trifluoromethylbenzaldehyde

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