tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate

Base Information

• Chemical Name: tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate
• CAS No.: 1356347-39-1
• Molecular Formula: C₂₅H₃₄N₆O₂
• Molecular Weight: 450.584
• Mol file: 1356347-39-1.mol

Synonyms:tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate

Chemical Property of tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate

There total 1 articles about tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

tert-butyl 4-((6-(methylthio)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate (1350550-48-9) + N,N-dimethylammonium chloride (506-59-2) → tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate (1356347-39-1)

Guidance literature:

tert-butyl 4-((6-(methylthio)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 2h;

N,N-dimethylammonium chloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 60 ℃; for 16h;

DOI:10.1021/ml200239k

Reference yield:

tert-butyl 4-((6-(dimethylamino)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate (1356347-39-1) → C20H26N6 + C20H26N6

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/ml200239k

upstream raw materials:

tert-butyl 4-((6-(methylthio)-3-phenyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate

N,N-dimethylammonium chloride