diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

Base Information

Chemical Name:diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate
CAS No.:1205743-69-6
Molecular Formula:C₃₂H₅₀N₆O₁₀P₂
Molecular Weight:740.731
Hs Code.:

Synonyms:diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

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Technology Process of diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

There total 1 articles about diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1205743-49-2
ethyl 2-(diethoxyphosphoryl)-2-methylpent-4-ynoate

: 102437-80-9
1,3-bis(azidomethyl)benzene

: 1205743-69-6
diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1055/s-0029-1216982

Reference yield: 78.0%

: 1205743-69-6
diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

: 1205743-71-0
diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-dihydroxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate

Guidance literature:: diethyl 2,2'-(1,1'-{1,3-phenylenebismethylenebis[2-methyl-2-diethoxyphosphoryl-3-(1H-1,2,3-triazol-4-yl)]})bispropanoate; With trimethylsilyl bromide; In chloroform; at 20 ℃; for 72h;

With water; In methanol;
DOI:10.1055/s-0029-1216982