10-CARBOXYDECYL DISULFIDE

Base Information

• Chemical Name: 10-CARBOXYDECYL DISULFIDE
• CAS No.: 23483-56-9
• Molecular Formula: C22H42 O4 S2
• Molecular Weight: 434.705
• Hs Code.: 2930909090
• Mol file: 23483-56-9.mol

Synonyms:Undecanoicacid, 11,11'-dithiodi- (6CI,8CI); 11,11'-Dithiobis[undecanoic acid];Bis(10-carboxydecyl) disulfide

Chemical Property of 10-CARBOXYDECYL DISULFIDE

Chemical Property:

• Melting Point: 93-97 °C
• Boiling Point: 594.4±15.0 °C(Predicted)
• PKA: 4.48±0.10(Predicted)
• PSA: 125.20000
• Density: 1.063±0.06 g/cm3(Predicted)
• LogP: 7.55880
• Storage Temp.: 2-8°C

Purity/Quality:

95%-98% ^*data from raw suppliers

Bis(10-carboxydecyl)disulfide 99% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10-CARBOXYDECYL DISULFIDE

There total 4 articles about 10-CARBOXYDECYL DISULFIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

11-mercaptounadecanoic acid (71310-21-9) → 11-(10'-carboxy-decyldisulfanyl)undecanoic acid (23483-56-9)

Guidance literature:

With sulfuryl dichloride; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/chem.201101027

Reference yield: 87.0%

11-bromoundecanoic acid (2834-05-1) → 11-(10'-carboxy-decyldisulfanyl)undecanoic acid (23483-56-9)

Guidance literature:

With benzyltriethylammonium tetrathiomolybdate; sodium carbonate; In water; at 25 ℃; for 17h;

DOI:10.1080/00397919708005447

Reference yield:

C11H21O5S2(1-)*Na(1+) → 11-(10'-carboxy-decyldisulfanyl)undecanoic acid (23483-56-9)

Guidance literature:

With hydrogenchloride; thiourea; In ethanol; Yield given; Heating;

DOI:10.1039/cc9960001193

upstream raw materials:

11-bromoundecanoic acid

11-mercaptounadecanoic acid

Downstream raw materials:

N-(4-azidophenyl)-11,11'-disulfanediyldiundecanoic amide

N-(4-ethynylphenyl)-11,11'-disulfanediyldiundecanoic amide

(4-{10-[10-(4-methoxycarbonylmethoxy-benzyloxycarbonylamino)-decyldisulfanyl]-decylcarbamoyloxymethyl}-phenoxy)-acetic acid methyl ester

11-[10-(4-nitro-phenoxycarbonyl)-decyldisulfanyl]-undecanoic acid 4-nitro-phenyl ester

Refernces

• 1、 Naka, Kensuke,Itoh, Hideaki,Chujo, Yoshiki. "Self-assembly of gold nanoparticles utilizing a charge-transfer interaction between carbazolyl and dinitrophenyl units". . p. 501 - 505. Retrieved 2005.
• 2、 -. "Redox-responsive micromolecular gel compound, preparation method thereof, micromolecular gel of compound and application thereof". Paragraph 0019; 0044-0045. . Retrieved 2021/02/10.
• 3、 Sóti, Péter Lajos,Yamashita, Hiroki,Sato, Kohei,Narumi, Tetsuo,Toda, Mitsuo,Watanabe, Naoharu,Marosi, Gy?rgy,Mase, Nobuyuki. "Synthesis of a self-assembling gold nanoparticle-supported organocatalyst for enamine-based asymmetric aldol reactions". . p. 1984 - 1990. Retrieved 2016/04/05.