33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene

Base Information

• Chemical Name: 33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene
• CAS No.: 84011-89-2
• Molecular Formula: C₄₃H₄₈N₆O₆
• Molecular Weight: 744.891

Synonyms:33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene

Chemical Property of 33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene

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Technology Process of 33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene

There total 1 articles about 33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3-(methoxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.12,6.17,11.113,17.119,23.124,28>octaconta-34(2),3,5,36(13),14,16,38(24),25,27-nonaene (84011-90-5) → 33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.12,6.17,11.113,17.119,23.124,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene (84011-89-2)

Guidance literature:

With hydrogen bromide; sodium carbonate; acetic acid; Yield given. Multistep reaction; 1.) 25 deg C, 20 min, 2.) 100 deg C, H₂O;

DOI:10.1021/ja00339a035

Reference yield: 34.0%

33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.12,6.17,11.113,17.119,23.124,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene (84011-89-2) + L-alanine 4-nitrophenyl ester perchlorate (84011-92-7) → L-alanine 33,35,37-trioxo-34,38-dimethoxy-4,15,26-trimethyl-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.12,6.17,11.113,17.119,23.124,28>octaconta-34(2),3,5,36(13),14,16,38(24),25,27-nonaene-36-yl ester perchlorate (84027-48-5)

Guidance literature:

With pyridine; In dichloromethane; at 25 ℃; for 48h;

DOI:10.1021/ja00329a059

Reference yield:

33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3(hydroxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.12,6.17,11.113,17.119,23.124,28>octaconta-34(2),3,5,36(13),14,16,38(24)25,27-nonaene (84011-89-2) + L-alanine 4-nitrophenyl ester perchlorate (84011-92-7) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + L-alanine 33,35,37-trioxo-34,38-dimethoxy-4,15,26-trimethyl-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.12,6.17,11.113,17.119,23.124,28>octaconta-34(2),3,5,36(13),14,16,38(24),25,27-nonaene-36-yl ester perchlorate (84027-48-5)

Guidance literature:

With diisopropylethylamine-perchlorate salt buffer; In chloroform-d1; at 24 ℃; Rate constant; concentration dependence, other nucleophiles;

DOI:10.1021/ja00339a035

upstream raw materials:

33,35,37-trioxo-34,38-dimethoxy-4,26-dimethyl-36-<3-(methoxymethyl)phenyl>-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24),25,27-nonaene

Downstream raw materials:

4-nitro-phenol

L-alanine 33,35,37-trioxo-34,38-dimethoxy-4,15,26-trimethyl-1,7,11,19,23,29-hexaazaheptacyclo<27.3.1.1^2,6.1^7,11.1^13,17.1^19,23.1^24,28>octaconta-34(2),3,5,36(13),14,16,38(24),25,27-nonaene-36-yl ester perchlorate

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