5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

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Chemical Name:5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile
CAS No.:931410-18-3
Molecular Formula:C₃₁H₃₂Cl₂N₂O₂
Molecular Weight:535.513
Hs Code.:

Synonyms:5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

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Chemical Property of 5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

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Technology Process of 5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

There total 6 articles about 5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 931410-10-5
methanesulfonic acid 1-(4-cyano-1,1-dimethyl-4,4-diphenylbutyl)azetidi-3-yl ester

: 931410-17-2
5-allyloxy-2,4-dichlorophenol

: 931410-18-3
5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/jm200884j

Reference yield: 93.0%

: 931410-18-3
5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

Guidance literature:

Reference yield:

: 521267-13-0
tert-butyl 4,4-dimethyl-1,2,3-oxathiazinane-3-carboxylate 2,2-dioxide

: 931410-18-3
5-[3-(5-allyloxy-2,4-dichlorophenoxy)azetidin-1-yl]-5-methyl-2,2-diphenylhexanenitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

1.2: 4.25 h / 20 °C / Inert atmosphere

1.3: 2 h / 50 °C / Inert atmosphere

2.1: sodium carbonate / dichloromethane; water

2.2: 18 h / 70 °C / Inert atmosphere

3.1: pyridine / 3.25 h / -15 - 5 °C / Inert atmosphere

4.1: potassium carbonate / acetonitrile / 3.5 h / 80 °C / Inert atmosphere

With pyridine; potassium tert-butylate; sodium carbonate; potassium carbonate; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1021/jm200884j